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Brookfield AMETEK

Laundry Detergent

Laboratory Viscometer Application Data Sheet

USE

To be used in washing machines to help clean clothes.

Test Equipment

  • Instrument: Powder Flow Tester (PFT)
  • Trough: 230 cc, 6-inch diameter
  • Lid Type: Vane Lid, 304 s/s, 33cc, 6-inch diameter (Flow Function)
    Wall Lid, 304 s/s, 2B finish, 6-inch diameter (Wall Friction)
  • Type of Test: Flow Function Test, Wall Friction Test
  • Temperature: Room Temperature (70-72° F)
  • Humidity: 48%

Method

A Brookfield Powder Flow Tester, equipped with Powder Flow Pro software for automated instrument control and data acquisition, was used to test this name brand laundry detergent. The laundry detergent was scooped into the trough, and the scraping tool was then used to evenly distribute the powder throughout the trough. After recording the sample weight and entering it into the software, a standard flow function test and then a wall friction test were run. Time required for each test was 35 minutes and 20 minutes respectively.

Parameters Measured

  • Flowability: Cohesive to Easy Flowing
  • Wall Friction: 25° to 17°
  • Bulk Density: 700 kg/m (fill density) to 930 kg/m

Analysis

  • Hopper Shape: Conical
  • Arching Flow Factor: 1.40
  • Critical Arching Dimension: 2.055 inches (52.2 mm)
  • Rathole Diameter: Dependent on bin diameter

Results


Figure 1: Laundry Detergent Flow Function Graph

Figure 1 shows the flowability of the laundry detergent at different levels of consolidating stress. These results show that the laundry detergent is generally easy flowing except at very low levels of consolidating stress (under 1 kPa).

Note: The Flow Function data is indicated by the red line. The other lines are references (or "Standard Flow Indices"), which distinguish the different types of flow behavior, ranging from "non-flowing" to "free flowing".


Figure 2: Laundry Detergent Wall Friction Graph

Figure 2 represents the angles of wall friction at different levels of normal stress. Angles of wall friction represent the friction between the sliding powder and the wall of the hopper or chute at the onset of flow. In this test a stainless steel lid was used, illustrating what the friction would be like if the laundry detergent was in a stainless steel hopper. At a low normal stress of about .5 kPa, the effective angle of wall friction is about 25 and goes down to about 17 at higher levels of normal stress (4.75 kPa).


Figure 3: Laundry Detergent Bulk Density Graph

Figure 3 shows the bulk density of the material at different levels of consolidating stress. This graph tells us that the detergent has a fill density of about 700 kg/m and rises to about 940 kg/m at around 9 kPa of consolidating stress. In general, a free flowing powder will show very small changes in bulk density, while a cohesive or poor flowing powder will generally show a large increase in bulk density.

Conclusion

The laundry detergent is a cohesive powder at low consolidation stress levels and an easy flowing at high consolidation stress levels. This means that the laundry detergent may have flowability issues as the hopper empties. Possible problems include arching (when the powder forms a cohesive bridge over the outlet) and ratholing (when the powder flows out only from the center leaving the rest of the material static against the walls). The critical arching dimension, of 2.055 inches (52.2 mm) provides a conservative estimate to prevent arching from happening, provided the minimum outlet dimension of the hopper exceeds this value. The critical ratholing dimension is dependent on the diameter of the bin. The rathole diameter can be automatically calculated by Powder Flow Pro once the bin diameter is entered.